< Back
Informasi Alat
| Nama Alat | Nuclear Magnetic Resonance (NMR) 400 Mhz |
|---|---|
| Deskripsi Alat | HIGH PERFORMANCE DIGITAL 400 MHZ NMR SPECTROMETER Brand : Bruker Model : AVANCE NEO 400 MHz NMR spectrometer Country of Origin : Switzerland Spesification : HIGH PERFORMANCE DIGITAL NMR SPECTROMETER Bruker Shim and Sample Transfer System Bruker high performance matrix Orthogonal Shim System (BOSS™) with 20 gradients (BOSS-1), low current and low heat dissipation design for optimum homogeneity. Bruker standard bore Sample Transfer (BST) system for sample insertion into the magnetic centre. Prepared for shim system cooling. Allows spinning of samples with 3 to 10mm sample diameter. Built-in sample down detection together with BSVT. Basic system characteristics The AVANCE NEO system console electronics is housed within a stainless steel RF 19-inch rack mounted one bay or double bay cabinet with full RF shielding (e.g. immunity against DVB-T, ATSC, ISDB-T and DTMB). The cabinet offers enough space to incorporate various 19-inch high power RF amplifiers depending on application and configuration. It incorporates a state-of-the-art Ethernet ROUTER providing up to 14 TCP/IP based Ethernet ports for internal and external spectrometer devices such as automatic sample changers, CryoProbe™ platforms, magnet control and monitoring equipment, solid state NMR accessories, etc. The system is equipped with a Power Distribution Unit (PDU) to allow software controlled console power-up and power-down via TopSpin™ . A dedicated, on-system Embedded Processing Unit (EPU) with separate 1TB Hard Disk drive allows versatile and flexible spectrometer control. Acquisition (AQS) characteristics · 80 MHz system clock, synchronicity on all channels within 12.5ns · A Timing and Gradient Control Unit (GTU) for all gradient amplifiers. It controls the overall timing of system (all RF channels, gradients, real time pulses, triggers, etc.) · Up to 8 Transceiver units (TRX1200). Each TRX1200 provides a full broad banded transmit and a full broad banded receive channel up to 1.2 GHz. See other TRX1200 specifications below. · Gradient control with a resolution of 12.5ns for Z and XYZ gradients (option) · Pulse program synchronization with up to 4 Trigger inputs at 12.5ns resolution (e.g. for high speed MAS rotor synchronization @111kHz) · NMR synchronized and real-time control output of external devices (e.g. laser systems, pumps). Up to 11 independent controls with 12.5ns resolution Bruker Smart Magnet control System (BSMS) supports · Ultra-stable shim current sources (SCB20) for Bruker RT shim systems · Optional Ethernet based Bruker Digital NMR Lock (2G DigiLock™) for 2H and/or 19F nuclei (L-TRX, L-19F) together with ultra-stable, ultra-low noise B0 current source (ELCB) · Bruker Smart Variable Temperature control (BSVT) controls with up to 4 independent VT channels, optional Bruker SmartCoolers™ (e.g. BCU-I), optional Low Temperature accessories (LN2 exchanger / evaporator) and High Temperature equipment · 10A High Resolution NMR gradient amplifiers (GAB/2, optional) · NMR Sample Transport for Bruker standard and wide bore magnet sample transport systems (BST) Systems equipped with 2G DigiLock™ and SmartVT™ support intrinsically the unique Bruker NMR Thermometer™ (e.g. to monitor and regulate the sample temperature within the sample tube). High performance and high power preamplifier system (HPPR) · Multi-receive ready up to 8 receiver channels. No extra wiring or other component required · Stray field compliant touch screen based human machine interface (HMI). Easy magic angle setup on the probe · RF power supervision for fast shut downs built-in (probe safety together with PICS) · Accurate tuning and matching with factory calibrated preamplifiers (Network analyzer technology) and fully integrated automatic tuning and matching (with ATM probe). No separate unit needed · Supports up to 8 RF preamplifiers Include AH0070 Helium Transfer Line Standard Helium Transfer Line AH0078 100l Nitrogen dewar 100L liquid Nitrogen dewar for use with CryoProbe Prodigy or magnet system. Nitrogen Gas Separator Membrane Nitrogen Separator, for production of >98% nitrogen from compressed air. Requires higher volumes of compressed than standard installation. MAGASC400SB Ascend 400 Magnet ASCEND™ 400 MHz/54 mm Long Hold Time Magnet superconducting magnet system, 54 mm bore - operation field at 9.4 Tesla - strayfield: radial 0.5m / axial 1.0m - helium hold time >300 days - helium level meter with alarm function for low helium level - nitrogen level sensor - standard magnet stand with elastomer vibration damping accessory Advanced magnet design, for significant reduction of the stray field and cryogen consumption. Incorporates External Disturbance Suppression (EDS™) for dramatic reduction of the effects of magnetic field perturbations from sources such as subways and electric trains. AH0068 Upgr. to Vibr. Damping 3Hz Upgrade of vibration dampers to Fabritech isolators with 3Hz natural resonance for Ascend 400 and 500MHz magnet systems with F-Version stand. Nitrogen refill set The corrugated plastic tubing is especially designed for nitrogen refilling. It's available as set 3 meters long and provided with two small (5 cm) pieces of silicon tubing that fit to the nitrogen inlet ports. SHIM CURRENT BOARD (SCB20) The SCB20 high precision, ultra-stable shim current board provides 20 shim current sources with each 20Bit digital resolution and +/- 1A shim current range. Depending on shim system type two units might be necessary. The current sources are compatible with all Bruker Orthogonal and Matrix shim systems (e.g. BOSS-3). Shim System Upgrade BOSS-1 to BOSS-3 Shim System Upgrade BOSS-1 to BOSS-3 10A GRADIENT AMPLIFIER (GAB/2) The GAB/2 is a fast single channel offset free gradient amplifier unit for pulsed field gradient shimming and single axis gradient enhanced spectroscopy (GRASP). It provides pulsed field gradients up to 10A (50ms per second) and a built-in pre-emphasis. On-axis (Z) and off-axis (XYZ) gradient shimming using real-time shim current control together with TopShimTM for single axis gradient probes. TopShimTM proprietary gradient shimming including lineshape optimization; see JMR 182(1), 38-48, 2006. Triple axis pulsed field gradient (XYZ) operation requires three GAB/2 units (option). 1H GaAs PREAMPLIFIER (HPLNA 1H) Highly linear, low noise, GaAs based preamplifier for 1H and 19F observe and decoupling with • Noise Figure (NF) ~1dB including all internal filters and active transmit-receive switch • Max. 4kW peak power RF capability • Build in RF power detection • Factory calibrated for accurate tuning and matching BB19F GaAs PREAMPLIFIER (HPPR XBB19F 2HP) Linear, low noise, GaAs based broad banded preamplifier for observe and decoupling of nuclei from 57Fe up to 19F with • Noise Figure (NF) ~1.4dB including all internal filters and active transmit-receive switch • Max. 500W peak power RF capability • Factory calibrated for accurate tuning and matching • Built-in 1H stop filter This broad banded RF preamplifier module is designed to be used with broad banded probes. 2H LOCK TRANSCEIVER (L-TRX) Integrated lock RF transceiver (L-TRX, transmit and receive unit) with incorporated 5W RF amplifier for field lock operation on deuterated solvents provides · Fast and accurate gradient shimming on 2H together with TopShimTM · Easy and reliable locking on multiple lock signal solvents (e.g. Pyridine) even in automation · Accurate sample temperature determination with NMR ThermometerTM TopShimTM proprietary gradient shimming including lineshape optimization; see JMR 182(1), 38-48, 2006. Can be extended with separate 19F lock option. 2H GaAs PREAMPLIFIER (HPPR 2H) Linear, low noise, GaAs based preamplifier for 2H observe, decoupling and lock operation with • Noise Figure (NF) ~1.4dB including all internal filters and active transmit-receive switch • Max. 500W peak power RF capability • 2H lock / observe RF routing built-in • Fast, pulse program controlled mode switching (lock / decouple) • Factory calibrated for accurate tuning and matching This highly selective module is designed to be used for selective probes without the need of external filters. 2H-Stop Filter 2H-Stop Filter TopSpin4 acquisition and processing licence TopSpin 4 acquisition and processing license including: - NMR data acquisition (arbitrary dimensions) and processing (1D, 2D, 3D, 4D and 5D) - TopGuide, menu guided acquisition setup - NMRGuide for training of users in use of 1D and 2D experiments with NMR literature library - Icon NMR automation interface Structure Analysis Software: - Relaxation analysis (T1/T2) - integration of 1D and 2D spectra - deconvolution of 1D and 2D spectra - NMRSIM for experiment simulation - Daisy spectrum simulation software - TopSpin interactive and automatic multiplet analysis - TopSpin solid state lineshape analysis - TopSpin integrated structure editor - CMC-assist, supporting NMR Data Interpretation - SmartDriveNMR for fully automated structure verification on the spectrometer 24 inch TFT MONITOR 24 inch TFT MONITOR Acquisition PC with Windows OS HP Windows 10 Pro 64Bit PC equipped according to latest configuration: e.g. HP Z440 Intel Xeon E5-1620v4 3.8GHz, Quad Core 16 GB RAM, 2TB Hard Disc DVD +/-RW DL Drive HP USB Laser Mouse (configuration may change without prior notice) PROBE VT ADAPTER THERMOCOUPLE TYPE T The VT adapter TC-2T provides two thermocouple type T sensor channels and one heater channel for corresponding NMR probes. It also connects to the heater safety sensor to prevent the probe from overheating in case of missing VT gas. VARIABLE TEMPERATURE CONTROL (BSVT) The Bruker SmartVT (BSVT) is a highly integrated unit to provide • Digital temperature sensor resolution better than 5mK • Temperature stability depends on environment and probe (e.g. 10mK/K for HR RT probes) • Supports various temperature sensor types (e.g. thermocouple T or E, PT100) • VT gas flow monitoring up to 3000lph with mass flow regulation • Anti-freeze mode for CryoProbes built-in (probe safety) • Up to 4 independent heater channels (e.g. flow probes) • High temperature measurements ready (up to 600°C with high temperature probes), no separate heater (booster) needed • Intelligent VT gas flow control for easy sample insertion with different kind of spinners (ceramic, KEL-F, etc.). No manual adjustments needed (e.g. SampleCase, SampleJet) • Intelligent SmartCoolersTM (BCU) and low temperature accessories control (LN2 exchanger/evaporator) • Accurate Sample Temperature determination and regulation with NMR ThermometerTM 2CH RF AMPLIFIER (BLABBH500/100) Linear 2 channel RF amplifier for observe and decoupling with • Min. 100W RF peak power @180 – 600 MHz (max. 25W CW) • Min. 500W RF peak power @15 – 600 MHz (max. 50W CW) Pulse program controlled blanking and ultra-fast rise/fall times. The broad band RF channel provides two identical RF outputs connecting to different preamplifiers when appropriate (no manual re-wiring). Built-in computer controlled RF amplifier safety with forward / reflected RF power monitoring. Ethernet interface for service and NMR system integration. RF CHANNEL (TRX1200) The TRX1200 is a highly integrated NMR RF transceiver (transmit and receive) unit with built-in pulse program engine (sequencer, waveform memory) providing • RF signal bandwidth of 5 to 1200 MHz for transmit and receive • Timing resolution of 12.5 ns • Simultaneous RF amplitude, phase & frequency setting within 12.5ns • High speed ADC, 240 MSPS @16 Bit, Digital Down Converter (DDC) • High speed DAC, 960 MSPS, Digital Up Converter (DUC) • High intermediate frequency (IF) for transmit and receive of 1852 MHz (e.g. no unwanted LO windows) • Sequencer waveform memory 1GB (e.g. pulse shaping, optimal control applications, composite pulse decoupling) • Spectral width up to 7.5 MHz • Effective dynamic range >17 Bit (5 MHz) / >19 Bit (1 MHz) / >23 Bit (6 kHz) CRPN2-DR-BB/1H&19F-5mm-EZ 5mm X-nuclei optimized double resonance cryo probe designed for X-nuclei observation with 1H decoupling and 1H observation with X-nuclei decoupling (ProdigyTM). The X-nuclei range includes31P-15N with the excluded region between 199Hg and 153Eu. Probe includes cooled preamplifiers for 1H(19F), 31P-15N range and 2H. 1H-circuit is tunable to 19F. Features (BBO H&F BBO-H-D-05 Z): · 2H lock · VT range -40°C to +80°C · Z gradient with 6 G/A*cm · Automated tuning & matching (ATM) BH5410 Cryo Platform PRODIGY N2-Cryo-Platform for Prodigy probe, cryo cooling unit with pumps; 2m of length (standard), basic system; 100 l dewar for 12 days; control electr.; on initial order of new system only BH5450 Balance for N2 level SHAT400A CMC-se ACA New CMC-se Structure Elucidation Software license for TopSpin3, based on MS input (molecular formula) and 1D/2D NMR data; to generate an editable correlation matrix between atoms; autom. peak picking and automation assisted Structure ELUcidation Note: requires TS3.1 (or higher) processing software, for WINDOWS and LINUX, password only - Academia AH0171 SampleCase Features: - Convenient sample access at user height - Safe operation - 24 easily accessed sample positions - Random access for sequential- or batch automation - Unique manual push-button sample exchange - Supports all common sample-tubes in spinners or shuttles - Compatible with MAS and CryoFIT Type A Kel-F Spinner standardbore shimsystems (5 mm) Type A Spinner Plastic (Kel-F) - selected quality for use 500MHz and higher 5 mm, standardbore, Tmax = 120°C 300 NMR-Tubes with code - Routine NMR, economy - 5 mm 600 MHz - Coded caps with NO holes Tubes for high throughput NMR, 5x178 mm (7 inch) 5 mm, outer diameter length 178 mm, wall 0.38 mm, camber 60 um, unit with 100 pcs including Bruker caps with code, up to 600 MHz. Do not use with Ceramic spinners. AssureNMR Software for Metabolomics Application (Free 1 Year) Additional application software package for individual projects to providing definitive answers to molecular questions at least as below : Can analyze different material types from mixtures to pure materials such as Metabolomics, NMR fingerprinting, Dietary supplements, APIs Quantification analysis of Multiple components and error analysis Spectral Assignments and databases Identify components Full automation from acquisition through analysis and reporting and fully customizable Statistic and chemometric such as PCA analysis, SIMCA outlier, quantile plot, PLS regression Application include: Quality control, Polymers, Food/Beverage, Pharmaceuticals, Natural products Fully integrated software and hardware solution to follow standard operating procedures (SOPs) and providing optimal reproducibility. AutoCalibration Include : 1. Free Cyrogen For 5 Yeas - Helium gas - Nitrogen gas - Liquid Helium - Liquid Nitrogen - Solvent NMR 2. Local Supply - AC - UPS - IsoTrans - Compressor - Installation, Training & Comissioning 3. Bruker FT- IR ALPHA II 4. Radleys Carousel 6 plus Standard system 5. Radleys Carousel 12 plus Standard system |
| Preparasi Sample | |
| Lokasi | Labtek XV |
| PIC | Dr. Aep Patah |
| Status | Active : Penggunaan Alat dapat dilakukan oleh semua users. |
| Waktu Penggunaan Alat | Per-jam |
